A simple method for synthesis and isolation of single PCB congeners shown by the example of PCB 132, a possible interference of PCB 153 and PCB 105

Publikations-Art
Zeitschriftenbeitrag
Autoren
Vetter, W.; Luckas, B.; Haubold, W.
Erscheinungsjahr
1991
Veröffentlicht in
Chemosphere
Band/Volume
23/2
Seite (von - bis)
193-8
Abstract

PCB 132 was prepd. by Cadogan coupling and isolated by semi-preparative reversed-phase HPLC in purity larger than 98%. The gas chromatog. sepn. of the PCBs 153, 132, and 105 on different silica fused columns (Ultra-2, HP-5, OV-1701, OV-210, OV-225) was discussed.

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